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CTRI Number  CTRI/2024/03/063933 [Registered on: 11/03/2024] Trial Registered Prospectively
Last Modified On: 27/02/2024
Post Graduate Thesis  Yes 
Type of Trial  Interventional 
Type of Study   Dentistry 
Study Design  Randomized, Parallel Group, Active Controlled Trial 
Public Title of Study   Regeneration of damaged enamel by application of a peptide 
Scientific Title of Study   Clinical evaluation of biomimetic self assembling peptide in remineralization of early buccal carious lesion - A Randomized Control Trial. 
Trial Acronym  NIL 
Secondary IDs if Any  
Secondary ID  Identifier 
NIL  NIL 
 
Details of Principal Investigator or overall Trial Coordinator (multi-center study)  
Name  Harini J Raj 
Designation  PG student - Master of Dental Surgery 
Affiliation  VS Dental college and hospital 
Address  6,Department of Conservative dentistry and Endodontics, VS Dental college and Hospital, KR Road, VV Puram

Bangalore
KARNATAKA
560004
India 
Phone  7339279150  
Fax    
Email  harinijraj@gmail.com  
 
Details of Contact Person
Scientific Query
 
Name  Dr. R.Anitha Kumari 
Designation  Professor and HOD 
Affiliation  VS Dental college and hospital 
Address  6,Department of Conservative Dentistry and Endodontics, VS Dental College and Hospital, KR Road, VV Puram

Bangalore
KARNATAKA
560004
India 
Phone  9845919324  
Fax    
Email  anithamanasi18@gmail.com  
 
Details of Contact Person
Public Query
 
Name  Harini J Raj 
Designation  PG student - Master of Dental Surgery 
Affiliation  VS Dental college and hospital 
Address  6,Department of Conservative Dentistry and Endodontics, VS Dental College and Hospital, KR Road, VV Puram

Bangalore
KARNATAKA
560004
India 
Phone  7339279150  
Fax    
Email  harinijraj@gmail.com  
 
Source of Monetary or Material Support  
VS Dental College and Hospital 
 
Primary Sponsor  
Name  Harini J Raj 
Address  VS dental college and hospital 6,Department of conservative dentistry and endodontics KR Road,VV puram Bangalore - 560004 
Type of Sponsor  Other [self] 
 
Details of Secondary Sponsor  
Name  Address 
NIL  NIL 
 
Countries of Recruitment     India  
Sites of Study  
No of Sites = 1  
Name of Principal Investigator  Name of Site  Site Address  Phone/Fax/Email 
Dr Harini J Raj  VS Dental College and Hospital  6,Department of conservative dentistry and endodontics, KR road , VV Puram Bangalore -560004
Bangalore
KARNATAKA 
7339279150

HARINIJRAJ@GMAIL.COM 
 
Details of Ethics Committee  
No of Ethics Committees= 1  
Name of Committee  Approval Status 
KEMPEGOWDA INSTITUTE OF MEDICAL SCIENCES INSTITUITIONAL ETHICAL COMMITTEE  Approved 
 
Regulatory Clearance Status from DCGI  
Status 
Not Applicable 
 
Health Condition / Problems Studied  
Health Type  Condition 
Patients  (1) ICD-10 Condition: K026||Dental caries on smooth surface,  
 
Intervention / Comparator Agent  
Type  Name  Details 
Comparator Agent  NANOHYDROXYAPATITE   10% aqueous slurry of nanohydroxyapatite is applied topically and left undisturbed for 3 mins. Applied only once and followed up at 1,3 and 6 months.  
Intervention  P11-4 PEPTIDE AND NANOHYROXYAPATITE  0.5mg of the p11-4 peptide is mixed with 0.05ml of sterile water and 10% aqueous slurry of nanohydroxyapatite, applied topically and left undisturbed for three minutes. Applied only once and followed up at 1,3 and 6 months. 
 
Inclusion Criteria  
Age From  18.00 Year(s)
Age To  60.00 Year(s)
Gender  Both 
Details  Teeth selection:
Surfaces included: buccal
Subjects with ≥1 visible and accessible early caries lesion present, which did not require operative intervention.
Patient selection:
Age group:18–60years
Had to provide written informed consent prior to any study procedures and needed to be able and willing to observe good oral hygiene throughout the study duration

 
 
ExclusionCriteria 
Details  Subjects receiving the following medications were excluded from the study: tetracyclines, any other medication known to stain teeth.

Subjects who are pregnant and breast feeding should be excluded from the study

Subjects who has evidence of reduced salivary flow or excessive tooth wear.

Subjects >1 carious lesion on the selected teeth
 
 
Method of Generating Random Sequence   Computer generated randomization 
Method of Concealment   Sequentially numbered, sealed, opaque envelopes 
Blinding/Masking   Participant, Investigator and Outcome Assessor Blinded 
Primary Outcome  
Outcome  TimePoints 
remineralization of early buccal carious lesion  1,3 and 6 months 
 
Secondary Outcome  
Outcome  TimePoints 
improved oral hygiene
improvement in aesthetics 
1,3 and 6 months 
 
Target Sample Size   Total Sample Size="40"
Sample Size from India="40" 
Final Enrollment numbers achieved (Total)= "Applicable only for Completed/Terminated trials"
Final Enrollment numbers achieved (India)="Applicable only for Completed/Terminated trials" 
Phase of Trial   Phase 3 
Date of First Enrollment (India)   23/03/2024 
Date of Study Completion (India) Applicable only for Completed/Terminated trials 
Date of First Enrollment (Global)  Date Missing 
Date of Study Completion (Global) Applicable only for Completed/Terminated trials 
Estimated Duration of Trial   Years="0"
Months="6"
Days="0" 
Recruitment Status of Trial (Global)   Not Applicable 
Recruitment Status of Trial (India)  Not Yet Recruiting 
Publication Details   N/A 
Individual Participant Data (IPD) Sharing Statement

Will individual participant data (IPD) be shared publicly (including data dictionaries)?  

Response - NO
Brief Summary  

Enamel caries is a progressive subsurface demineralisation ultimately resulting in mechanical failure and cavitation.

For “early” carious lesions, the currently used treatment protocol include sealing carious lesions (sealants and resin infiltration), and remineralization procedures mainly with fluorides or using CPP-ACP ,to determine whether or not the lesion will progress, in which case a restoration would then be placed

When the ph of saliva is critically low at 5.5 the presence of additional extrinsic sources of stabilized Ca2+ and PO43– ions could augment the natural remineralization potential of saliva by increasing diffusion gradients favouring faster and deeper subsurface remineralization.

The shift from repairative to regenerative dentistry reflects the current trend in medicine wherein diseased dental tissues are replaced with biologically similar tissues

Enamel regeneration is however particularly challenging as mature enamel is acellular and does not resorb or remodel itself unlike bone or dentin.

Advances in tissue engineering methods have yielded biomimetic methods that have demonstrated a strong potential for regenerating the hierarchical enamel microstructure. The novel rationally designed self-assembling P11-4 peptide,consisting of 11 amino acids  can be used  for regenerating  demineralized tooth tissue .

This low viscosity isotropic P11-4 when applied on the initial carious lesion rapidly diffuses into the lesion body, where it transforms to an elastomeric nematic gel in the presence of cations and pH < 7.4, leading to the 3-dimensional fibre matrix assembly ,which enables de novo hydroxyapatite crystal formation facilitating the  guided enamel regeneration of the lost enamel structure.

Aim of the study is To compare the combinatory effects of novel self assesmbling p11-4 peptide and nanohydroxyapatite  with that of nanohydroxyapatite alone on remineralization efficacy of early buccal carious lesions. 

 OBJECTIVES OF THE STUDY

To assess the  remineralization efficacy following  a single application of  P11-4 and nanohydroxyapatite mixture on early buccal surface enamel lesions.

To assess the remineralization efficacy following  application of nanohydroxyapatite alone on early buccal surface lesions.

To compare the p11-4 peptide – nanohydroxyapatite mixture with that of nanohydroxyapatite alone on the basis of  remineralization efficacy.

SOURCE OF SUBJECTS:

40 outpatients attending the Department of Conservative Dentistry and Endodontics from Vokkaligara Sangha Dental College, Bangalore, who will have volunteered to participate will be included in the study.

MATERIALS INCLUDED IN THE STUDY

P 11 -4 PEPTIDE

nanohydroxyapatite

Prophylaxis paste.

Etching agent.

Sterile water.

Applicator tip.

Micromotor.

Exploratory probe.

Digital camera.

     Rubber dam kit

BASELINE ASSESSMENT:

A general oral and physical examination including a dental, medical and social history.

 A series of digital colour photographs of the test lesion taken under standard conditions of light and magnification.

 A detailed relevant medical (including dental) history covering the previous three years and a medication they were taking at the time of the study.

 

PROCEDURE FOR APPLICATION OF P11-4 PEPTIDE

After recording preoperative condition, isolation is achieved using rubber dam.

The superficial pellicle is removed by using a prophylaxis paste such as pumice, followed by application of 35% phosphoric acid for 30 s.

After cleaning and drying surface is assessed for open pores to allow the material to penetrate the lesion and initiate the process.

Lyophilized  p11-4 peptide is rehydrated with 0.05 ml of sterile water and a single drop of the resulting solution is immediately applied on the lesion for  approximately 5mins ensuring moisture control.10% aqueous slurry of nanohydroxyapatite is applied and left undisturbed for 3 mins.

For the control group the same procedure is repeated  adding nanohydroxyapatite alone

FOLLOW UP

The patient will be assessed and evaluated at baseline,1, 3 & 6 months after treatment using standard digital photographs, Nyvad score.

ASSESMENT OF THE LESION:

A series of colour photographs of the test lesion is taken under standard conditions of light and magnification to asses lesion size, appearance and progression.

A chart and professional photographs is made for each patient for follow up and scoring of the white spot lesions at different time periods.

The clinical photographs are processed using photographic editing software (Adobe Photoshop 7.0, Adobe Systems Inc., San Jose, California, USA), then the stained area is calculated as % of the total teeth area by the following equatio

The data is subjected to analysis at baseline, 3 and 6 months respectively.

SCORING CRITERIA – NYVAD SCORING CRITERIA

Score

CATEGORY

CRITERIA

0

Sound

Normal enamel translucency & texture(slight staining allowed in otherwise sound fissure)

1

Active caries

(intact surface)

Surface of enamel is white/ yellowish opaque with loss of lustre; feels rough when the tip of the probe is moved gently across the surface ;generally covered with plaque.

No clinically detectable loss of substance.

Smooth surface; carious lesions typically located near the gingival margin.

Fissure/pit: intact: lesion extending along the walls of the fissure,

2

Active caries

(surface discontinuity)

 

Same criteria as score 1

Localized surface defect( microcavity) in enamel only.

No undermined enamel or softened floor detectable with the explorer.

3

Active caries

(cavity)

Enamel/dentin cavity easily visible with the naked eye: surface of cavity feels soft or leathery on

gentle probing

There may or may not be pulpal involvement.

4

Inactive caries

(intact surface0

Surface of enamel is whitish, brownish or black

Enamel may be shiny and feels hard

and smooth when the tip of the probe is moved

gently across the surface

no clinically detectable loss of substance

Smooth surface caries lesion

typically located at some distance from gingival margin

Fissure/pit:intact fssure morphology: lesion extending along, the walls of the fissure

5

Inactive caries

(surface discontinuity)

Same criteria as score

-Localized surface detect (microcavity, in enamel only

No undermined enamel or softened floor detectable with the explorer.

 

6

Inctive  caries

(cavity)

Enamel /dentin cavity easilv visible with the naked eye, surface of cavity mav be shinv and feels

hard on probing with gentle pressure.

No  pulpal involvement

 

7

Filling (sound surface)

 

 

8

Filling + active caries

Caries lesion may be cavitated or non cavitated.

 

9

Filling + inactive caries

Caries lesion may be cavitated or non cavitated.

 

ANALYSIS OF DATA

Statistical Package for Social Sciences [SPSS] for Windows Version 22.0 Released 2013. Armonk, NY: IBM Corp., will be used to perform statistical analyses.

Descriptive Statistics:

Descriptive analysis of all the explanatory and outcome parameters will be done using mean and standard deviation for quantitative variables, frequency and proportions for categorical variables.

Inferential Statistics:

Chi Square Test will be used to compare the Nyvad criteria for assessment for the Buccal Lesions & Success Rate treated between biomimetic self-assembling peptide P11-4-nanohydroxyapatite mixture with that of nanohydroxyapatite alone at 3 & 6 Months’ post follow-up period.

Marginal Homogeneity test will be used to compare the Nyvad criteria for assessment for the Buccal Lesions between 3 & 6 Months’ post follow-up period in each study group.

McNemar’s test will be used to compare the mean success rate of remineralization of buccal lesions between 3 & 6 Months’ post follow-up period in each study group.

The level of significance will be set at P<0.05.

            And any other relevant test, if found appropriate during the time of data analysis will be dealt accordingly.

 
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