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CTRI Number  CTRI/2025/04/084767 [Registered on: 15/04/2025] Trial Registered Prospectively
Last Modified On: 15/04/2025
Post Graduate Thesis  Yes 
Type of Trial  Interventional 
Type of Study   Dentistry 
Study Design  Randomized, Parallel Group, Active Controlled Trial 
Public Title of Study   Assessing a Special Tooth Repair Material (Calcium Silicate-Doped Dentin) for Treating Deep Cavities While Keeping the Tooth Alive 
Scientific Title of Study   Comparative evaluation of calcium silicate-doped treated dentin matrix and mineral trioxide aggregate as miniature pulpotomy biomaterials in deep carious lesions: a parallel, double-blind, randomized clinical trial 
Trial Acronym  nil 
Secondary IDs if Any  
Secondary ID  Identifier 
NIL  NIL 
 
Details of Principal Investigator or overall Trial Coordinator (multi-center study)  
Name  Dr Muhammad Hamdan 
Designation  Junior Resident 
Affiliation  All India Institute of Medical Sciences, Nagpur 
Address  Department of Dentistry, AIIMS Nagpur, Mihan, Nagpur

Nagpur
MAHARASHTRA
441108
India 
Phone  9900772357  
Fax    
Email  hmmden26@gmail.com  
 
Details of Contact Person
Scientific Query
 
Name  Prof Dr Ganesh Jadhav 
Designation  Associate Professor 
Affiliation  All India Institute of Medical Sciences, AIIMS Nagpur 
Address  Room no.407, OPD Building, 4th Floor, Department of Dentistry, All India Institute of Medical Sciences, Mihan, Nagpur

Nagpur
MAHARASHTRA
441108
India 
Phone  9823649979  
Fax    
Email  drganesh2009aiims@gmail.com  
 
Details of Contact Person
Public Query
 
Name  Prof Dr Ganesh Jadhav 
Designation  Associate Professor 
Affiliation  All India Institute of Medical Sciences, AIIMS Nagpur 
Address  Room no.407, OPD Building, 4th Floor, Department of Dentistry, All India Institute of Medical Sciences, Mihan, Nagpur

Nagpur
MAHARASHTRA
441108
India 
Phone  9823649979  
Fax    
Email  drganesh2009aiims@gmail.com  
 
Source of Monetary or Material Support  
Self Funded (Institute of study: AIIMS Nagpur) 
 
Primary Sponsor  
Name  Muhammad Hamdan 
Address  Department of Dentistry, AIIMS Nagpur, Mihan, Nagpur, 441108 
Type of Sponsor  Other [Self Funded] 
 
Details of Secondary Sponsor  
Name  Address 
NIL  NIL 
 
Countries of Recruitment     India  
Sites of Study  
No of Sites = 1  
Name of Principal Investigator  Name of Site  Site Address  Phone/Fax/Email 
Dr Muhammad Hamdan  All India Institute of Medical Sciences, Nagpur  4th Floor, OPD building, AIl India Institue of Medical Sciences, Mihan, Nagpur
Nagpur
MAHARASHTRA 
9900772357

hmmden26@gmail.com 
 
Details of Ethics Committee  
No of Ethics Committees= 1  
Name of Committee  Approval Status 
Institutional Ethics Committee, Department of Pharmacology, AIIMS Nagpur  Approved 
 
Regulatory Clearance Status from DCGI  
Status 
Not Applicable 
 
Health Condition / Problems Studied  
Health Type  Condition 
Patients  (1) ICD-10 Condition: K040||Pulpitis,  
 
Intervention / Comparator Agent  
Type  Name  Details 
Intervention  Miniature Pulpotomy using calcium silicate- doped Human treated dentin matrix (hTDM) as a medicament  hTDM will be placed as a medicament over vital pulp tissue after caries excavation. The patient will be assesed after 7 days and for 1, 3, 6 months to assess the vitality of the tooth and absence of clinical symptoms and any radiographic changes 
Comparator Agent  Miniature Pulpotomy using Mineral Trioxide Aggregate (MTA) as a medicament  MTA will be placed as a medicament over vital pulp tissue after caries excavation. The Patient will be assesed after 7 days and for 1,3,6 months to assess the vitality of the tooth and absence of clinical signs and symptoms and any radiographic changes. 
 
Inclusion Criteria  
Age From  14.00 Year(s)
Age To  35.00 Year(s)
Gender  Both 
Details  Clinical diagnosis of reversible pulpitis.
Positive response to pulp sensibility tests.
Normal periapical tissues (PAI index less or equal to 2).
Presence of carious lesion involving three fourth or entire thickness of dentin. (Deep or extremely deep carious lesions) 
 
ExclusionCriteria 
Details  History of spontaneous unprovoked pain
Pain on percussion, sinus tract, swelling, excessive mobility.
Periodontal pockets greater than 4 mm.
Presence of a crack.
Profuse hemorrhage from exposure site (greater than 5 minutes)
Presence of serous or purulant exudates from exposure site.
Teeth with traumatic occlsuion, non carious lesions, developmental defects.
Radiographic evidence of internal or external resorption, calcifications, condensing osteitis or furcal and periapical radiolucency. 
 
Method of Generating Random Sequence   Computer generated randomization 
Method of Concealment   Sequentially numbered, sealed, opaque envelopes 
Blinding/Masking   Participant and Outcome Assessor Blinded 
Primary Outcome  
Outcome  TimePoints 
Pulp Vitality assessed by Cold Testing  7 days, 3 months, 6 months 
 
Secondary Outcome  
Outcome  TimePoints 
Post operative Pain using NRS-11 scale  24, 48, 72 hours and 7 days. 
Presence or absence of Swelling, sinus tract  7 days, 3 months, 6 months 
Presence or absence of Tenderness on percussion  7 days, 3months, 6 months 
Pocket depth (mm)  7 days, 3 months, 6 months 
Mobility (Grading)  7 days, 3 months, 6 months 
Radiographic outcome: Periapical Index (PAI) score  7 days, 3 months, 6 months 
Presence or absence of resorption (Internal/External)  7 days, 3 months, 6 months 
 
Target Sample Size   Total Sample Size="56"
Sample Size from India="56" 
Final Enrollment numbers achieved (Total)= "Applicable only for Completed/Terminated trials"
Final Enrollment numbers achieved (India)="Applicable only for Completed/Terminated trials" 
Phase of Trial   N/A 
Date of First Enrollment (India)   03/05/2025 
Date of Study Completion (India) Applicable only for Completed/Terminated trials 
Date of First Enrollment (Global)  Date Missing 
Date of Study Completion (Global) Applicable only for Completed/Terminated trials 
Estimated Duration of Trial   Years="1"
Months="6"
Days="0" 
Recruitment Status of Trial (Global)   Not Applicable 
Recruitment Status of Trial (India)  Not Yet Recruiting 
Publication Details   N/A 
Individual Participant Data (IPD) Sharing Statement

Will individual participant data (IPD) be shared publicly (including data dictionaries)?  

Response - YES
  1. What data in particular will be shared?
    Response - All of the individual participant data collected during the trial, after de-identification.

  2. What additional supporting information will be shared?
    Response -  Study Protocol
    Response -  Statistical Analysis Plan
    Response - Informed Consent Form
    Response - Clinical Study Report

  3. Who will be able to view these files?
    Response - Anyone

  4. For what types of analyses will this data be available?
    Response - Any purpose.

  5. By what mechanism will data be made available?
    Response - Data are available indefinitely at (Link to be included hmmden26@gmail.com).

  6. For how long will this data be available start date provided 30-04-2025 and end date provided 30-01-2035?
    Response - Immediately following publication. No end date.

  7. Any URL or additional information regarding plan/policy for sharing IPD? 
    Additional Information - NIL
Brief Summary  

SUMMARY OF THE STUDY

Comparative evaluation of calcium silicate-doped treated dentin matrix and

mineral trioxide aggregate as a novel miniature pulpotomy biomaterials in

deep carious lesions: a parallel, double-blind, randomized clinical trial

Rationale of the study:

Vital pulp therapies have become common in recent years in part due to the

development of highly biocompatible materials like MTA and various

formulations of calcium silicate based materials. Calcium hydroxide based pulp

therapies have nearly been replaced by MTA. MTA and calcium silicates are

now recognized as the benchmark for vital pulp therapies.

Recently, Treated dentin matrix, an extracellular matrix-based biomaterial, has

emerged as an excellent scaffold for tissue engineering because of its

remarkable biological induction activity, distinct natural structure, and

biocompatibility. In addition to having a high level of bioactivity, a treated

dentin matrix can work as a transporter for bioactive substances and medication

molecules, aiding in the processes of tissue regeneration and

immunomodulation. Similar products such as demineralized bone matrices

(DBMs) and other allograft bone materials have already found their place in

clinical practice.

AIM:

To develop a Novel calcium silicate-doped human-treated dentin matrix

(CaSi+hTDM) to assess its potential as a Miniature Pulpotomy (MP)

biomaterial.

OBJECTIVES:

Primary objective:

To evaluate the efficacy of calcium silicate-doped human-treated dentin matrix

(CaSi+hTDM) compared to Mineral Trioxide Aggregate (MTA) in maintainingpulp vitality using cold testing following Miniature Pulpotomy (MP) in deep

and extremely deep carious lesions with reversible pulpitis

Secondary objectives:

1. To evaluate patient-reported outcomes such as pain, swelling, sinus tract etc.

post-operatively.

2. To determine the clinical success rates of both materials by assessing the

Periapical index of healing over a 1-year follow-up period.

Type of study: Randomized controlled trial

Duration of study: 18 months

Sample size:

According to the study by Bogen et al the success rate for Direct pulp capping

using MTA was 98%. Given the lack of specific evidence on the success rate

for Direct Pulp Capping (DPC) using calcium silicate-doped human-treated

dentin matrix (CaSi+hTDM) and since Miniature pulpotomy is a modification

of DPC, it was assumed that the success rate for CaSi+hTDM would not be

lower than that of MTA. Using a 20% non-inferiority limit, 80% precision of

the test, and 5% type I error rate, the required sample size was calculated to be

44 teeth per material group. To account for potential dropouts, 20% was added

to the required sample size, resulting in a final sample size of 98 teeth.

Inclusion criteria

 Patient age 14 -35 years.

 Noncontributory medical history (ASA1 and 2)

 Deep and extremely deep caries

 Vital mature teeth with symptoms of reversible pulpitis.

 Positive response to pulp sensibility testing.

 Clinical diagnosis of reversible pulpitis with PAI score less than or equal to 2.

 Tooth should be restorable

 Pocket depth and mobility should be within normal limits. (less than 4mm)

Exclusion criteria:

 Immature roots

 Clinical signs of pulp necrosis such as swelling or presence of sinus tract

 Prominent radiolucency in the furcation area, presence of internal or

external root resorption, any calcification, and any periapical lesion. No evidence of bleeding after exposure.

 Profuse hemorrhage from exposure site. (greater than 10minutes)

 History of spontaneous unprovoked pain, pain on percussion

 Presence of serous or purulent exudates from exposure site.

Fabrication of Calcium silicate doped-human treated dentin matrix (CaSi +

hTDM):

Human molars will be removed from patients for clinical reasons under ethical

approval. Periodontal and dental pulp tissue and enamel will be completely stripped

away to obtain dentin. The resulting dentin matrix will then be perforated and soaked

in deionized water for 5 hours and mechanically cleaned for 20 minutes every hour

using an ultrasonic cleaner. Human dentin matrices are then soaked in 17% Ethylene

Diamine Tetra-acetic Acid (EDTA) for 5 mins, washed in deionized water for 10 mins

in an ultrasonic cleaner, exposed to 10% EDTA for 5 mins, and washed in deionized

water for 10 mins in an ultrasonic cleaner, exposed to 5% EDTA for 10 mins, washed

in deionized water for 10 mins in an ultrasonic cleaner. To eliminate organic content,

teeth will be immersed in isopropanol for 2 hours. Samples will be stored in saline

solution in a refrigerator until milling is done to get a fine powder. A homogenizer will

be used for 5 mins at 1440 RPM.

Treatment procedure:

After Local anaesthesia administration, rubber dam isolation is done, the operative field

and the tooth will be disinfected using 5% sodium hypochlorite (NaOCl) prior to caries

excavation. A round diamond bur will be employed, along with a spoon excavator, to

thoroughly remove the soft caries under magnification. To confirm the intra-operative

pulp vitality, the presence of bleeding at the exposed pulp will be confirmed. Removal

of pulp tissue not exceeding 1 mm in depth. Haemostasis will be achieved by the

application of a pellet moistened with 2.5% NaOCl for 1 min with a dry pellet on topand repeated if required for up to 5 min. After controlling the bleeding, MTA or CaSi

doped hTDM will be applied over the pulp.

The post treatment clinical evaluation will be performed at 24, 48 and 72 hours, 3, 6

and 12 months.

Radiographic evaluation will be done at 3, 6,12 months.

Statistical Analysis:

The data will be entered in Epidata Manager v.4.4.6.0.6 [Odense, Denmark]. The data

will be cleaned and analysed using Epi Analysis. We will check the normality of the

data using Shapiro Wilk and Kolmogorov Smirnov test. Depending on the normality

continuous data will be described as mean ± standard deviation (± SD) or median and

interquartile range where appropriate. For parametric data, independent sample t-test

will be used to compare between two groups in non-related samples for baseline

comparison. For non-parametric data, Mann Whitney test will be used to compare

between two groups in non-related samples for baseline comparison. Chi square

test/Fischer’s exact test will be used to compare for proportions between intervention

and control arms. The change in outcomes between the two groups will be compared

using two-way ANOVA. The proportions will be reported with 95% confidence

interval. The statistical significance level will be set at P less than or equal to 0.05

 
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