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CTRI Number  CTRI/2026/01/101146 [Registered on: 14/01/2026] Trial Registered Prospectively
Last Modified On: 08/01/2026
Post Graduate Thesis  Yes 
Type of Trial  Interventional 
Type of Study   Drug
Dentistry 
Study Design  Randomized, Parallel Group Trial 
Public Title of Study   Comparative evaluation of clinical and radiographic outcome of 3 indirect pulp capping materials in primary teeth: A Randomized Clinical Trial 
Scientific Title of Study   Comparative evaluation of clinical and radiographic outcome of MTA, THERACAL LC, and 3MIXTATIN as indirect pulp capping material in primary teeth: A Randomized Clinical Trial 
Trial Acronym   
Secondary IDs if Any  
Secondary ID  Identifier 
NIL  NIL 
 
Details of Principal Investigator or overall Trial Coordinator (multi-center study)  
Name  Dr. Jaya Bhangdiya 
Designation  Post Graduate Student 
Affiliation  Swargiya Dadasaheb Kalmegh Smruti Dental College and Hospital, Nagpur 
Address  DEPARTMENT OF PEDIATRIC AND PREVENTIVE DENTISTRY, SECOND FLOOR, 202, SWARGIYA DADASAHEB KALMEGH SMRUTI DENTAL COLLEGE AND HOSPITAL, NAGPUR

Nagpur
MAHARASHTRA
441110
India 
Phone  8888335373  
Fax    
Email  jayabhangdiya9108@gmail.com  
 
Details of Contact Person
Scientific Query
 
Name  Dr. Milind Wasnik 
Designation  READER AND PROFESSOR 
Affiliation  Swargiya Dadasaheb Kalmegh Smruti Dental College and Hospital, Nagpur 
Address  DEPARTMENT OF PEDIATRIC AND PREVENTIVE DENTISTRY, SECOND FLOOR, 202, SWARGIYA DADASAHEB KALMEGH SMRUTI DENTAL COLLEGE AND HOSPITAL, NAGPUR
SANGAM ROAD WANADONGRI
Nagpur
MAHARASHTRA
441110
India 
Phone  8888335373  
Fax    
Email  milind.wasnik@sdk-dentalcollege.edu.in  
 
Details of Contact Person
Public Query
 
Name  DR JAYA BHANGDIYA 
Designation  Post Graduate Student 
Affiliation  Swargiya Dadasaheb Kalmegh Smruti Dental College and Hospital, Nagpur 
Address  DEPARTMENT OF PEDIATRIC AND PREVENTIVE DENTISTRY, SECOND FLOOR, 202, SWARGIYA DADASAHEB KALMEGH SMRUTI DENTAL COLLEGE AND HOSPITAL, NAGPUR

Nagpur
MAHARASHTRA
441110
India 
Phone  8888335373  
Fax    
Email  jayabhangdiya9108@gmail.com  
 
Source of Monetary or Material Support  
SWARGIYA DADASAHEB KALMEGH SMRUTI DENTAL COLLEGE AND HOSPITAL,NAGPUR 441110 INDIA 
 
Primary Sponsor  
Name  Dr Jaya Bhangdiya 
Address  SWARGIYA DADASAHEB KALMEGH SMRUTI DENTAL COLLEGE AND HOSPITAL NAGPUR,INDIA 441110 
Type of Sponsor  Other [Self] 
 
Details of Secondary Sponsor  
Name  Address 
NIL  NIL 
 
Countries of Recruitment     India  
Sites of Study  
No of Sites = 1  
Name of Principal Investigator  Name of Site  Site Address  Phone/Fax/Email 
Dr Jaya Bhangdiya  Swargiya Dadasaheb Kalmegh Smruti Dental College and Hospital Nagpur  Second, 202, Department of Pediatric and Preventive Dentistry, Swargiya Dadasaheb Kalmegh Smruti Dental College and Hospital Nagpur
Nagpur
MAHARASHTRA 
8888335373

jayabhangdiya9108@gmail.com 
 
Details of Ethics Committee  
No of Ethics Committees= 1  
Name of Committee  Approval Status 
INSTITUTIONAL ETHICAL COMMITTEE  Approved 
 
Regulatory Clearance Status from DCGI  
Status 
Not Applicable 
 
Health Condition / Problems Studied  
Health Type  Condition 
Patients  (1) ICD-10 Condition: K029||Dental caries, unspecified,  
 
Intervention / Comparator Agent  
Type  Name  Details 
Comparator Agent  3 MIXTATIN  a combination of metronidazole, minocycline, and ciprofloxacin (3Mix) has been used as an endodontic material regarding the concept of lesion sterilization and tissue repair (LSTR) therapy. 3Mix is capable of eliminating bacterial pathogens from infected dental tissues in both permanent and primary dentitions. It has provided an excellent outcome in indirect pulp therapy of primary molars. We propose the term 3Mixtatina, an acronym for mixture of 3Mix and simvastatin, for the new combination. This novel combination was applied with the aim of suppressing bacteria, preventing pulp inflammation, and inducing hard tissue formation. Moreover, the effect of 3Mix and simvastatin alone was assessed separately[1:1:1:1][metronidazole: ciprofloxacin: minocycline : simvastatin] 
Intervention  MTA  ProRoot MTA is a biomaterial that has been investigated for endodontic applications since the early 1990s. Despite its many advantages, MTA has some drawbacks such as a long setting time and discoloration potential, among others. Hence, efforts have been made to overcome these shortcomings, new calcium silicate-based bioactive restorative cement has been developed, namely biodentine. Advantages of this material are short setting time, high compressive and flexural strength, and color stability along with ease of manipulation. manipulation in a ratio 1:1 [liquid: powder] 
Comparator Agent  Theracal LC  TheraCal LC is a single paste calcium silicate-based material promoted by the manufacturer for use as a pulp capping agent and as a protective liner for use with restorative materials, cement, or other base materials. This material has been classified as a 4th generation calcium silicate material. According to ISO 9917-2017 part 2 clause 4.1, TheraCal LC is a class 2 cement material which the setting reaction of the polymerizable component is light-activated.  
 
Inclusion Criteria  
Age From  3.00 Year(s)
Age To  8.00 Year(s)
Gender  Both 
Details  1. On clinical examination, deep carious lesion involving occlusal and proximal surfaces or multi surfaces with the gingiva appearing normal in primary second molars.
2. Mild discomfort from chemical and thermal stimuli.
3. History of dull, intermittent, but bearable pain associated with eating.
4. Restorable by a stainless-steel crown (SSC).
5. Radiographically, more than two-thirds of dentin thickness is being involved by caries approaching the pulp with intact lamina dura and periodontal ligament (PDL) space appearing normal.
6. Radiographically more than two-thirds of the root is present, with no periapical changes, and no pathologic external or internal resorption or necrosis.
7. Cooperative children and parents willing to follow the instructions and report for follow-up.
 
 
ExclusionCriteria 
Details  1. Acute pulpal inflammation and necrosis indicated by a history of sharp penetrating pulpalgia, tenderness on percussion, and prolonged spontaneous pain at night.
2. Clinically, mobile tooth, discolored tooth, and a tooth with sinus opening, fistula, or abscess.
3. Radiographically, interrupted lamina dura, internal or external root resorption, inter radicular or periapical pathoses, and widened periodontal ligament space
4. Presence of chronic systemic diseases such as congenital or rheumatic heart disease, hepatitis, and leukemia
5. On long-term medication such as corticosteroid therapy
6. Physically or mentally challenged.
 
 
Method of Generating Random Sequence   Computer generated randomization 
Method of Concealment   Other 
Blinding/Masking   Open Label 
Primary Outcome  
Outcome  TimePoints 
To evaluate and compare the clinical and radiographic outcome of MTA, TheraCal LC and 3Mixtatin as Indirect pulp capping materials in Primary Teeth.  BASELINE, 3 MONTH AND 6 MONTH 
 
Secondary Outcome  
Outcome  TimePoints 
To Compare the clinical and radiographic outcome of MTA, TheraCal LC and 3Mixtatin as Indirect pulp capping materials in Primary Teeth.  after 3 month and 6 month 
 
Target Sample Size   Total Sample Size="60"
Sample Size from India="60" 
Final Enrollment numbers achieved (Total)= "Applicable only for Completed/Terminated trials"
Final Enrollment numbers achieved (India)="Applicable only for Completed/Terminated trials" 
Phase of Trial   Phase 3/ Phase 4 
Date of First Enrollment (India)   26/01/2026 
Date of Study Completion (India) Applicable only for Completed/Terminated trials 
Date of First Enrollment (Global)  Date Missing 
Date of Study Completion (Global) Applicable only for Completed/Terminated trials 
Estimated Duration of Trial   Years="2"
Months="0"
Days="0" 
Recruitment Status of Trial (Global)   Not Yet Recruiting 
Recruitment Status of Trial (India)  Not Yet Recruiting 
Publication Details   N/A 
Individual Participant Data (IPD) Sharing Statement

Will individual participant data (IPD) be shared publicly (including data dictionaries)?  

Response - NO
Brief Summary  

PRIMARY OBJECTIVE: To evaluate and compare the clinical and radiographic outcome of MTA, TheraCal LC and 3Mixtatin as Indirect pulp capping materials in Primary Teeth.

I) Study design: Randomized Clinical Trial

II) Study setting: The study will be conducted in the Department of Pedodontics and Preventive Dentistry

III) Study population: Primary second molar carious teeth in patients between 3 to 8 years old will be chosen for the study.

IV) Sample size estimation :

Sample size for estimating pre-post mean difference for an in-vivo study

Sample size  n= 17 per group.

Assuming 10% losses to follow up in the 6-month follow-up period, the effective sample size will be n = 17*(1/1-0.10) =18.87, say 20 per group.

Considering there will be 3 comparison groups, the total sample size requirement will be n = 20*3 =60.

Therefore, a total of 60 specimens will be included in this study.

Method Of Selection of Study Subjects: 

The ethical clearance will be obtained from the institutional ethical committee. A total of 60 primary second molar teeth from patients between 3 to 8 years old will be chosen for the study. The teeth will be allocated into three groups equally and randomly comprising 20 teeth in each group (Group I: MTA, Group II: light-cured calcium silicate - TheraCal LC, and Group III: 3Mixtatin) based on the following criteria.

 

Inclusion criteria : 

  1. On clinical examination, deep carious lesion involving occlusal and proximal surfaces or multi surfaces with the gingiva appearing normal in primary second molars.
  2. Mild discomfort from chemical and thermal stimuli.
  3. History of dull, intermittent, but bearable pain associated with eating.
  4. Restorable by a stainless-steel crown (SSC).
  5. Radiographically, more than two-thirds of dentin thickness is being involved by caries approaching the pulp with intact lamina dura and periodontal ligament (PDL) space appearing normal.
  6. Radiographically more than two-thirds of the root is present, with no periapical changes, and no pathologic external or internal resorption or necrosis.
  7. Cooperative children and parents willing to follow the instructions and report for follow-up.

 

Exclusion criteria :

1.      Acute pulpal inflammation and necrosis indicated by a history of sharp penetrating pulpalgia, tenderness on percussion, and prolonged spontaneous pain at night.

2.      Clinically, mobile tooth, discolored tooth, and a tooth with sinus opening, fistula, or abscess.

3.      Radiographically, interrupted lamina dura, internal or external root resorption, inter radicular or periapical pathoses, and widened periodontal ligament space

4.      Presence of chronic systemic diseases such as congenital or rheumatic heart disease, hepatitis, and leukemia

5.      On long-term medication such as corticosteroid therapy

6.      Physically or mentally challenged.

Withdrawal criteria: 

1.      Voluntary withdrawal at any point by participants.

2.      Accidental pulp exposure.

 

Method of Measurements: 

A complete case history of the patient will be taken. Patients will be evaluated randomly in different 3 Groups. This study will be conducted by using a randomized clinical trial. 60 children aged between 3 to 8 years will be selected using the random allocation sampling method.  

Each child’s parents or guardians will be explained in detail about the procedure in the local language (Marathi, Hindi or English). They will be informed about their right to refuse or discontinue their participation at any time and will be then asked to sign the consent form.

Study subjects will be randomly allocated into three groups: 

Group I: MTA (ProRoot, Dentsply/Tulsa Dental, Tulsa, OK, USA)

Group II: TheraCal LC ( Bisco Inc., Illinois, United States of America)

Group III: 3Mixtatin (Simvastatin, Metronidazole, Cefixime, Ciprofloxacin)

 

METHODOLOGY:

Before the procedure, a preoperative diagnostic radiograph of the tooth with a grid will be taken. Topical anesthesia will be applied first, following which local anesthesia will be administered, after which isolation will be achieved with a rubber dam. A two-step carious lesion removal procedure will be undertaken: (1) a high-speed round diamond bur will be used to remove carious enamel and dentin, and (2) a sharp spoon excavator will be used to curette the dentin manually only to remove the infected dentin. Care will be taken not to expose the pulp. Then, a pulp capping medicament will be selected and placed in the cavity after manipulating it by following the manufacturer’s instructions.

In group I, MTA ( ProRoot, Dentsply/Tulsa Dental, Tulsa, OK, USA)powder and sterile water will be mixed for 30 seconds (following the instructions of the manufacturer) until a sandy consistency is obtained, it will be carried with an MTA carrier in the prepared cavity and light pressure will be applied by a moist cotton pellet and then temporized.

In group II, using a dispensing syringe, light-cured calcium silicate (TheraCal lc®, Bisco IncIllinois, United States of America) will be applied to the dentin surface directly and will be light-cured for 20 seconds.

In group III, the 3Mixtatin will be prepared using three commercially available antibiotics metronidazole, ciprofloxacin, and cefixime along with simvastatin powder. After removal of the capsules or coating materials that enclosed the drug products, they will be pulverized to fine powders using porcelain mortars and pestles. A total of 100 mg of metronidazole, 100 mg of ciprofloxacin, and 100 mg of cefixime will be mixed in a 1:1:1 ratio, and 2 mg of simvastatin powder will be added to the final powdered drug mix, which will be kept in a tightly capped porcelain bottle. This powder will be mixed with Macrogol and Propylene Glycol to form a creamy paste.

For the permanent restoration in all three groups, Glass ionomer cement (Medicept Xtracem GIC TYPE II) will be first placed as a cavity base. The tooth will be then prepared for an SSC, which will be fixed with glass ionomer luting cement ( Medicept Xtracem GIC TYPE I)

Immediately, a baseline radiograph will be taken. Subsequently, the tooth will be examined clinically and radiographically in the 3rd and 6th month.

Clinically, treatment will be considered successful when there is an absence of the following: pain, sensitivity to pressure, abnormal tooth mobility, and abscess. The treatment will be radiographically considered successful when there is an absence of the following: furcation radiolucency, broken lamina dura, widening of PDL space and external and internal resorption of the root. The teeth will be evaluated clinically and radiographically at 3 and 6 months.

 

Additional points for Research in AYUSH

Not Applicable

 

Additional points for RCT

 i) Randomization:

The selected sample of 60 specimens will be randomly allocated to three groups using the Simple block randomization method. A predetermined, computer-generated random allocation plan will be utilized wherein 10 blocks of size 6 each will be used for equal assignment of specimens to all the comparison groups.

ii) Masking (Concealment):

The use of block randomization and unpredictable computer-generated random sequences will help in masking or concealment of treatment assignment to all the specimens.

iii) Blinding:

This is an Open-label randomized controlled trial where the investigator will be blinded to treatment assignment.

Additional points for all Experimental Studies

i) Explained intervention in required details

Before the procedure, a preoperative diagnostic radiograph of the tooth with a grid will be taken. Topical anesthesia will be applied first, following which local anesthesia will be administered, after which isolation will be achieved with a rubber dam. A two-step carious lesion removal procedure will be undertaken: (1) a high-speed round diamond bur will be used to remove carious enamel and dentin, and (2) a sharp spoon excavator will be used to curette the dentin manually only to remove the infected dentin. Care will be taken not to expose the pulp. Then, a pulp capping medicament will be selected and placed in the cavity after manipulating it by following the manufacturer’s instructions.

In group I, MTA ( ProRoot, Dentsply/Tulsa Dental, Tulsa, OK, USA)powder and sterile water will be mixed for 30 seconds (following the instructions of the manufacturer) until a sandy consistency is obtained, it will be carried with an MTA carrier in the prepared cavity and light pressure will be applied by a moist cotton pellet and then temporized.

In group II, using a dispensing syringe, light-cured calcium silicate (TheraCal lc®, Bisco IncIllinois, United States of America) will be applied to the dentin surface directly and will be light-cured for 20 seconds.

In group III, the 3Mixtatin will be prepared using three commercially available antibiotics metronidazole, ciprofloxacin, and cefixime along with simvastatin powder. After removal of the capsules or coating materials that enclosed the drug products, they will be pulverized to fine powders using porcelain mortars and pestles. A total of 100 mg of metronidazole, 100 mg of ciprofloxacin, and 100 mg of cefixime will be mixed in a 1:1:1 ratio, and 2 mg of simvastatin powder will be added to the final powdered drug mix, which will be kept in a tightly capped porcelain bottle. This powder will be mixed with Macrogol and Propylene Glycol to form a creamy paste.

For the permanent restoration in all three groups, Glass ionomer cement (Medicept Xtracem GIC TYPE II) will be first placed as a cavity base. The tooth will be then prepared for an SSC, which will be fixed with glass ionomer luting cement ( Medicept Xtracem GIC TYPE I)

Immediately, a baseline radiograph will be taken. Subsequently, the tooth will be examined clinically and radiographically in the 3rd and 6th month.

Clinically, treatment will be considered successful when there is an absence of the following: pain, sensitivity to pressure, abnormal tooth mobility, and abscess. The treatment will be radiographically considered successful when there is an absence of the following: furcation radiolucency, broken lamina dura, widening of PDL space and external and internal resorption of the root. The teeth will be evaluated clinically and radiographically at 3 and 6 months.

Duration: 18-24 months. 

 


 
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